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21.
《Journal of the European Ceramic Society》2019,39(16):5373-5379
The nanocrystals play a critical role in generating and affecting functionalities of glass materials. Therefore, scientists have made considerable efforts in clarifying microscopic mechanisms of nanocrystal formation in glass to obtain the desired type of nanocrystals. However, the phase transitions of nanocrystals during heating have not been well understood. Here we report on a discovery of the reversible melting-formation of nanocrystals in an oxyfluoride germanate glass during heating-cooling circles. Using a differential scanning calorimetry (DSC), we detected a striking endothermic event at 925 K during heating, after the glass underwent a DSC upscan to a temperature between 925–986 K and subsequent cooling. Based on Raman spectroscopy, X-ray diffraction and transmission electron microscopy, the endotherm is attributed to the melting of nano-crystal BaGeF6 (˜20 nm). An exothermal response was observed at 890 K during the DSC downscan, implying the re-formation of BaGeF6 nano-crystals. This suggests that the melting-formation of BaGeF6 nano-crystals is a typical first-order transition. 相似文献
22.
Catalysts of quaternary composition have been prepared and tested for the Sabatier process. For catalyst syntheses the following techniques have been used: sol‐gel methods, wet impregnation and incipient wetness impregnation. The Sabatier reaction was carried out at temperatures between 520 K and 670 K, pressures of 15 bar and 30 bar using a mixture H2:CO2 of 4:1. Activity screening of the microscale wall catalysts was performed by a custom‐built 10‐fold parallel gas‐flow microreactor setup in sequential operating mode. To analyze the gas phase compositions GC‐FID was used. 相似文献
23.
快循环同步加速器(RCS)是中国散裂中子源(CSNS)的重要组成部分。负氢粒子束经直线加速器加速至80 MeV,剥离成质子束注入至RCS环并加速累积至1.6 GeV引出打靶。束流通过安装在RCS环的壁电流探测器(WCM)感应得到束流的强度信息,环高频与环主二极磁铁的失配会导致束流的实际振荡偏离理论预测。本文通过对WCM的数据进行分析得到了纵向工作点、束流的实际振荡频率、束团的电荷量、束团的形状变化等信息,方便了加速器的调束,并对参数测量中的测量误差进行了分析。 相似文献
24.
This paper presents a field study of constructing retaining walls using soilbags that are formed by filling the excavated clayey soils into woven bags (geosynthetics). The strength and deformation of the soilbags filled with clayey soils were studied via laboratory tests. A 100?m testing retaining wall was constructed with soilbags in a waterway project. The lateral deformation, the lateral pressures and the surface settlements of the testing retaining wall were monitored during construction and after 7 months operation. The results show that the soilbags can increase the strength of clayey soils. After 7 months of the completion, the lateral deformation and the surface settlement of the testing retaining wall tend to be stable with the maximum values of 29.4?cm and 19.2?cm, respectively. The lateral earth pressure on the front retaining structure could be positively reduced owing to the interlayer's friction of soilbags. Compared to the conventional gravity concrete retaining wall, about 38% construction cost was saved in the 100?m testing retaining wall. 相似文献
25.
26.
《Geotextiles and Geomembranes》2020,48(2):157-169
A GeoBarrier system (GBS) is a combination system of reinforced soil walls to stabilize near-vertical cut slopes and capillary barrier principles to protect the wall from the effect of rainfall infiltration. Singapore requires construction materials that are cost-effective to support sustainable urban development. Therefore, recycled materials are utilized as GBS materials to avoid the use of high-cost materials, such as steel or concrete. GBS consists of planting geobags with unique geosynthetic pockets for sustainable plant growth as a facing layer of GBS. The negative pore-water pressure (suction) within the reinforced soil behind GBS was assured to be constant during rainfall since GBS is designed specially to minimize the rainfall infiltration into the reinforced soil. This paper presents the practical design and stability analysis of the GBS, considering the presence of suction within the reinforced soil body. The monitoring of GBS performance in the field was carried out via field instrumentation. Finite element analyses of the GBS under extreme rainfalls were also performed for evaluation of the GBS performance. The field instrumentations and numerical analysis results showed that GBS was able to protect the slope from rainfall infiltration; therefore, the stability of the slope retained by GBS was not affected by the rainfall. Results from the analytical calculation showed that the most critical mode of failure is sliding along the base, followed by the global and local slope stability. The GBS is not susceptible to local instability. 相似文献
27.
Abrasive jet micro-machining (AJM) uses compressed air carrying abrasive solid particles to micro-machine a variety of features into surfaces. If the feature sizes are less than the size of the abrasive jet footprint, then a patterned erosion-resistant mask is used to protect the substrate material, leaving exposed areas to define the features. Previous investigations have revealed a ‘blast lag’ phenomenon in which, for the same dose of abrasive particles, narrower mask openings lead to channels that are shallower than wider ones. Blast lag occurs when using AJM on brittle substrates because of the natural tendency to rapidly form a V-shaped cross-sectional profile which inhibits abrasive particle strikes on the narrow vertex at the feature centerline. In this paper, the blast lag phenomenon is studied when using AJM to machine a network of microfluidic channels. It is found that, in some cases, differences in blast lag occurring at channel intersections and within the channels themselves, can lead to channel networks of nonuniform depth. A previously developed surface evolution model is adapted to allow prediction of the onset of blast lag in the channels and intersections and thus explain these differences. Finally, methods to eliminate the differences are discussed. 相似文献
28.
装配式建筑相较于传统建筑,具有节能减排、绿色环保、快速施工、工业化生产和缩短工期等优势,能有效改善我国现阶段建筑业劳动力低、技术创新弱、建筑品质不高的局面,推动建造方式的改变,并能大幅提高企业信息化、可视化管控管理水平,并通过预制装配式产业链的整合,催生相关新产业和服务业,可以使产业链上各企业的核心竞争力得到提高。全产业标准化,规格化,使得信息流、资金流和物流得到有效整合。 相似文献
29.
Sherif M. Sharroush 《International Journal of Electronics》2018,105(12):2009-2032
As well known by computer architects, the performance gap between the processor and the memory has been increasing over the years. This causes what is known as the memory wall. In order to alleviate the problem, a novel fast readout scheme is proposed in this article for the single-transistor single-capacitor dynamic random-access memory (1T-1C DRAM) cells. The proposed scheme works in the current domain in which the difference between the discharging rates of the bitline in the cases of ‘1’ and ‘0’ readings is detected. The proposed scheme is analysed quantitatively and compared with the conventional readout scheme. It is verified by simulation adopting the 45 nm CMOS Berkley predictive-technology model (BPTM) and shows 44 and 7.7% reductions in the average read-access and cycle times, respectively, as compared to the conventional readout scheme. It is also shown that the power is saved according to the proposed scheme if the probability of occurrence of ‘0’ storage exceeds 66.7%. This minimum value can be alleviated, however, at the expense of a smaller saving in the average read-access time. The impacts of process variations and technology scaling are also taken into account. 相似文献
30.
《Ceramics International》2021,47(18):25997-26009
The effects of adding ZrO2 and TiO2 at the expense of MgF2 on the crystallization, microstructure, mechanical properties, thermal properties and electrical properties of mica glass-ceramics based on the SiO2–MgO–MgF2–K2O system were investigated by the differential scanning calorimetry (DSC), X-ray powder diffraction (XRD), scanning electron microscopy (SEM), microhardness tester and resistivity tester. The electrical properties were discussed emphatically. The results showed that the additions of ZrO2 and/or TiO2 at the expense of MgF2 effectively increase the viscosity, the glass transition temperatures (Tg) and the crystallization temperatures (Tp) of the glasses. The crystallization activation energy (Ec) of the amorphous glasses varied with the nucleating agents was discussed in depth. It was discovered that the nucleating agents had no effect on the crystal phase type but had a certain effect on the crystallinity and microstructure. Tetrasilicic fluoromica and enstatite were precipitated at different crystallization temperatures. Due to the non-stoichiometric ratio of tetrasilicic fluoromica crystal, the prepared glass-ceramics had high dielectric constant (24.4–34.3) and volume resistivity (>2 × 1011 Ω cm) at 25 °C, and the dielectric loss was almost zero. 相似文献